Potassium Hydroxide → HCID 15016268, compound

HRID 2106591Notes

Reaction equation

HRID 2106591 reaction equation
C([O:3][C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:19]=[CH:18][C:17]([O:20][CH3:21])=[CH:16][CH:15]=2)[N:10]=1)[CH3:7])=[O:5])C.[OH-].[K+]>C(O)C>[C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:15]=[CH:16][C:17]([O:20][CH3:21])=[CH:18][CH:19]=2)[N:10]=1)[CH3:7])([OH:5])=[O:3]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 15016250HCID 15016250, compound

Product 1

HCID 15016268HCID 15016268, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Four g of the compound of Example 8 was refluxed for 4 hours with 1.5 g of potassium hydroxide in 50 ml of ethanol, and the product was collected as shown in Example 22 and recrystallized from ethanol to obtain 2.6 g of the desired product, m.p. 155°-157°.

Workup

  1. customthe product was collected
  2. customrecrystallized from ethanol

Sources & evidence

ORD record
ord-105d050a6e464f7695f542a6907be0fa
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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