Potassium Hydroxide → HCID 15016273, compound

HRID 2106592Notes

Reaction equation

HRID 2106592 reaction equation
C([O:3][C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:19]=[CH:18][C:17]([CH3:20])=[CH:16][CH:15]=2)[N:10]=1)[CH3:7])=[O:5])C.[OH-].[K+]>C(O)C>[C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:15]=[CH:16][C:17]([CH3:20])=[CH:18][CH:19]=2)[N:10]=1)[CH3:7])([OH:5])=[O:3]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 15016253HCID 15016253, compound

Product 1

HCID 15016273HCID 15016273, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 2.5 g portion of the compound of Example 11 was refluxed for 4 hours with 1 g of potassium hydroxide in 50 ml of ethanol, and the product was collected as described in Example 22 to obtain 2.0 g of the desired product, m.p. 163°-165°.

Workup

  1. customthe product was collected

Sources & evidence

ORD record
ord-52ad12b4b8d54325ae9e235e188391ae
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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