HRID2106594

反应详情

EQUATION

反应方程式

HRID 2106594 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Ten g of the compound of Example 19 was refluxed for 10 minutes with 3.3 g of potassium hydroxide in 150 ml of ethanol, and the product was collected as described in Example 22 and recrystallized from ethanol to obtain 8.0 g of the desired product, m.p. 195°-197°.

WORKUP

后处理

  1. customthe product was collected
  2. customrecrystallized from ethanol