Dimethylamine → HCID 15016302, compound

HRID 2106620Notes

Reaction equation

HRID 2106620 reaction equation
[C:1]([CH:4]([O:6][C:7]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][CH:13]=2)[N:8]=1)[CH3:5])([OH:3])=O.[CH3:22][NH:23][CH3:24]>>[CH3:22][N:23]([CH3:24])[C:1]([CH:4]([O:6][C:7]1[N:11]=[CH:10][N:9]([C:12]2[CH:17]=[CH:16][C:15]([C:18]([F:21])([F:20])[F:19])=[CH:14][CH:13]=2)[N:8]=1)[CH3:5])=[O:3]

Participants

3

Reactant 2

HCID 674DimethylamineHCID 15016300HCID 15016300, compound

Product 1

HCID 15016302HCID 15016302, compound

Procedure

Three g of the product of Example 65 was reacted with 4 ml of 45% aqueous dimethylamine, substantially as shown in Example 60, to obtain 1.2 g of the desired product, m.p. 102°-104°.

Sources & evidence

ORD record
ord-e017ea8f9e194968a190a4ea20caa3c5
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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