Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2106686Generated: October 31, 2026

11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one → HCID 14369664, compound

https://huagongshe.com/reaction/2106686

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-oneHCID 14209983—
ReactantHCID 14369615HCID 14369615—
SolventAcetonitrileHCID 6342—
ProductHCID 14369664HCID 1436966458%

Reaction Steps

Prepared analogously to Example 4 from 11-(chlorocarbonyl)-6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one and 3-[3-(1-piperidinyl)propyl]piperidine in a yield of 58% of theory. Colourless crystals, m.p. 165.5°-167.0° C. (acetonitrile).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04931436
Source datasetuspto-grants-1990_06
ORD IDord-1af19703b5794c04b45a786a1f1bafe9
Source noteuspto-grants-1990_06