HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 14369650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one | HCID 11043962 | — |
| Reactant | 3-[4-(Diethylamino)butyl]piperidine | HCID 15057311 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14369650 | HCID 14369650 | 90% |
Reaction Steps
Prepared analogously to Example 1 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 3-[4-(diethylamino)butyl]piperidine in a yield of 90% of theory. Colourless crystals, m.p. 182°-184° C. (ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931436 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-2169fea6c0494dc1a54c9a6a80a482f4 |
| Source note | uspto-grants-1990_06 |