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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2106710Generated: November 1, 2026

11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one → HCID 15057336, compound

https://huagongshe.com/reaction/2106710

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-chlorocarbonyl-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-oneHCID 11043962—
ReactantHCID 15057335HCID 15057335—
SolventEthylacetate methanolHCID 21584119—
ProductHCID 15057336HCID 1505733613%

Reaction Steps

Prepared analogously to Example 4 from 11-(chlorocarbonyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]benzodiazepin-6-one and 3-[2-(diethylamino)ethyl]pyrrolidine in a yield of 13% of theory. Colourless crystals, m.p. 137°-138° C. (from ethyl acetate/methanol 98/2 v/v).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04931436
Source datasetuspto-grants-1990_06
ORD IDord-75e42214716c41078550d74f7ec5629d
Source noteuspto-grants-1990_06