Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 1-Naphthylamine | HCID 8640 | — |
| Reactant | 3-Fluoro-4-nitropyridin-1-ium-1-olate | HCID 594028 | — |
| Product | HCID 23049211 | HCID 23049211 | — |
Reaction Steps
To 1-naphthylamine (5.43 g) in 100 ml of absolute ethanol was added 3-fluoro-4-nitropyridine-N-oxide (6.0 g) in 25 ml of ethanol and this mixture was heated to 70° C. and stirred for six hours. The mixture was filtered to yield a solid (6.6 g) which was recrystallized from ethanol to yield a solid (2.6 g), m.p. 200°-201° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04931457 |
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| Source dataset | uspto-grants-1990_06 |
|---|
| ORD ID | ord-76b9118d760f46c0a5063562786b0612 |
|---|
| Source note | uspto-grants-1990_06 |
|---|
