Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-Naphthylamine | HCID 7057 | — |
| Reactant | 3-Fluoro-4-nitropyridin-1-ium-1-olate | HCID 594028 | — |
| Product | HCID 23049209 | HCID 23049209 | — |
Reaction Steps
To 150 ml of ethanol were added 3-fluoro-4-nitropyridine-N-oxide (7.0 g) and 2-aminonaphthalene (6.6 g) and the mixture was heated to 70° C. and stirred for one hour. The mixture was cooled and filtered and the solid collected to yield a solid (11.5 g). A 2.5 g portion of this material was triturated with methanol to yield a solid, 2.5 g, m.p. 222°-224° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04931457 |
|---|
| Source dataset | uspto-grants-1990_06 |
|---|
| ORD ID | ord-c18c4e6db80f4402bb606b77e3694693 |
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| Source note | uspto-grants-1990_06 |
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