3-Iodobenzyl alcohol → 3-Iodobenzaldehyde

HRID 2106878Notes

Reaction equation

HRID 2106878 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH2:5][OH:6].[Cr](Cl)([O-])(=O)=O.[NH+]1C=CC=CC=1.C([O-])(=O)C.[Na+]>>[I:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH:5]=[O:6]

Participants

4

Reactant 3

HCID 423003-Iodobenzyl alcoholHCID 517045Sodium AcetateHCID 178418287HCID 178418287, compound

Product 1

HCID 2526103-Iodobenzaldehyde

Procedure

3-iodobenzaldehyde was prepared by oxidation of 3-iodobenzylalcohol by pyridinium chlorochromate in the presence of sodium acetate as in Example 9.

Sources & evidence

ORD record
ord-7eb7c6cfca02400ea18b6a1a0413df85
Source dataset
uspto-grants-1990_06
Patent number
US04931469

Reaction notes

Loading…