1,2-Dichloro-3-iodobenzene → HCID 23049293, compound

HRID 2106881Notes

Reaction equation

HRID 2106881 reaction equation
C(O)CCC#C.ClC1C(Cl)=CC=CC=1I.[Cl:16][C:17]1[C:22]([Cl:23])=[CH:21][CH:20]=[CH:19][C:18]=1[C:24]#[C:25][CH2:26][CH2:27][CH:28]=[O:29]>>[Cl:16][C:17]1[C:22]([Cl:23])=[CH:21][CH:20]=[CH:19][C:18]=1[C:24]#[C:25][CH2:26][CH2:27][CH2:28][OH:29]

Participants

4

Reactant 3

HCID 754591,2-Dichloro-3-iodobenzeneHCID 793464-Pentyn-1-olHCID 23049339HCID 23049339, compound

Product 1

HCID 23049293HCID 23049293, compound

Procedure

5-(2',3'-dichlorophenyl)-4-pentyn-1-ol was prepared from 4-pentyn-1-ol and 2,3-dichloro-iodobenzene using the same method as in Example 15 and converted into 5-(2',3'-dichlorophenyl)-4-pentyn-1-al as in Example 9.

Sources & evidence

ORD record
ord-656e75d6894245b291a8c39f244908d8
Source dataset
uspto-grants-1990_06
Patent number
US04931469

Reaction notes

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