HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54000078, compound → HCID 54126786, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54000078 | HCID 54000078 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54126786 | HCID 54126786 | — |
Reaction Steps
26.6 g (0.0886 mol) of 3,5-dinitro-2-isopropylthiobenzoic acid methyl ester are dissolved in 270 ml of tetrahydrofuran and hydrogenated with the addition of 10 g of Raney nickel at from 30° to 35° C. The catalyst is then isolated by filtration, the filtrate is concentrated and the residue is crystallised from ethyl acetate/hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04931581 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-71bf037662c74c3a8e2bd464ba26ca75 |
| Source note | uspto-grants-1990_06 |