1,3-Dichloroacetone → HCID 14350368, compound

HRID 2106996Notes

Reaction equation

HRID 2106996 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[S:7])=[CH:4][CH:3]=1.[Cl:11][CH2:12][C:13]([CH2:15]Cl)=[O:14]>CC(C)=O>[ClH:1].[Cl:11][CH2:12][C:13](=[O:14])[CH2:15][S:7][C:6](=[NH:8])[C:5]1[CH:9]=[CH:10][C:2]([Cl:1])=[CH:3][CH:4]=1

Participants

4

Reactant 2

HCID 107931,3-DichloroacetoneHCID 27348264-Chlorothiobenzamide2×

Product 1

HCID 14350368HCID 14350368, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

8.58 g (50 mmol) of the 4-chlorothiobenzamide obtained in (a) were dissolved in 35 ml acetone, 6.35 g (50 mmol) of 1,3 dichloroacetone were added and left to stand for 1 day at room temperature. The crystallate was drawn off, washed with acetone and dried.

Workup

  1. waitleft
  2. washwashed with acetone
  3. customdried

Sources & evidence

ORD record
ord-5f0999d95f07436187086f711e12c6c2
Source dataset
uspto-grants-1990_06
Patent number
US04933328

Reaction notes

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