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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2107022Generated: October 31, 2026

Benzyl Bromide → HCID 15052395, compound

https://huagongshe.com/reaction/2107022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl BromideHCID 7498—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 14600605HCID 14600605—
SolventAcetoneHCID 180—
ProductHCID 15052395HCID 1505239571%

Reaction Steps

A suspension comprising 3.0 g of 8-(4-hydroxyphenyl)octanol, 3.0 g of anhydrous potassium carbonate, 50 ml of dry acetone and 1.9 ml of benzyl bromide was heated under reflux for 16 hours. After the completion of the reaction, the potassium carbonate was filtered off and the filtrate was concentrated on an evaporator. The white solid thus obtained was precipitated from chloroform-hexane (1:4). As a result, 3.0 g of the desired compound was obtained (yield: 71%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04933329
Source datasetuspto-grants-1990_06
ORD IDord-9253725bdc344fde96103dda4aa7da07
Source noteuspto-grants-1990_06