HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 15052395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 14600605 | HCID 14600605 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 15052395 | HCID 15052395 | 71% |
Reaction Steps
A suspension comprising 3.0 g of 8-(4-hydroxyphenyl)octanol, 3.0 g of anhydrous potassium carbonate, 50 ml of dry acetone and 1.9 ml of benzyl bromide was heated under reflux for 16 hours. After the completion of the reaction, the potassium carbonate was filtered off and the filtrate was concentrated on an evaporator. The white solid thus obtained was precipitated from chloroform-hexane (1:4). As a result, 3.0 g of the desired compound was obtained (yield: 71%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933329 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-9253725bdc344fde96103dda4aa7da07 |
| Source note | uspto-grants-1990_06 |