Thionyl Chloride → HCID 53915754, compound

HRID 2107075Notes

Reaction equation

HRID 2107075 reaction equation
[CH:1]([C:3]1([C:12]([OH:14])=O)[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2].S(Cl)([Cl:17])=O>>[CH:1]([C:3]1([C:12]([Cl:17])=[O:14])[CH2:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4]1)=[CH2:2]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 19828700HCID 19828700, compound

Product 1

HCID 53915754HCID 53915754, compound

Procedure

A mixture 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid (5.09 g) and thionyl chloride (25 ml) was refluxed for 10 hours. Excess thionyl chloride was distilled off under reduced pressure. The crude product was used as such for the following reaction.

Workup

  1. distillationExcess thionyl chloride was distilled off under reduced pressure
  2. customsuch for the following reaction

Sources & evidence

ORD record
ord-3181891f19eb44b699d84eb8b2c27787
Source dataset
uspto-grants-1990_06
Patent number
US04933359

Reaction notes

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