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HRID2107076

反应详情

EQUATION

反应方程式

HRID 2107076 的结构方程式

REACTANTS

反应物

3
结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：C=CC1(C(=O)Cl)Cc2ccccc2C1
HCID53915754

未命名化合物

结构：CCOC(=O)CC(=O)O.CCO[Mg]
HCID178472270

未命名化合物

PRODUCTS

生成物

1
结构：C=CC1(C(C)=O)Cc2ccccc2C1
HCID19828702

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCOCCCC
溶剂HCID8909

Butyl ether

C8H18O

PROCEDURE

实验过程

1-(2,3-Dihydro-2-vinyl-1H-inden-2-yl)-ethanone was prepared by treating 2,3-dihydro-2-vinyl-1H-indene-2-carboxylic acid chloride with ethoxy magnesium malonic acid ethyl ester in dibutylether and after that with sulfuric acid according to the method of Reynolds, G. A. and Hauser, C. B., Org. Synth. 30 (1957) 70.