HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Acetyl-3-hydroxy-2-propylbenzyl chloride → Ethyl 4-[[5-[(4-acetyl-3-hydroxy-2-propylbenzyl)thio]-1,3,4-thiadiazol-2-yl]thio]butyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Acetyl-3-hydroxy-2-propylbenzyl chloride | HCID 13781022 | — |
| Reactant | HCID 178471747 | HCID 178471747 | — |
| Product | Ethyl 4-[[5-[(4-acetyl-3-hydroxy-2-propylbenzyl)thio]-1,3,4-thiadiazol-2-yl]thio]butyrate | HCID 14373004 | 98.1% |
Reaction Steps
Using as starting materials 0.30 g of 4-acetyl-3-hydroxy-2-propylbenzyl chloride and 0.42 g of ethyl 4-[(5-mercapto-1,3,4-thiadiazol-2-yl]thio]butyrate, 0.59 g of oily ethyl 4-[[5-[(4-acetyl-3-hydroxy-2-propylbenzyl)thio]-1,3,4-thiadiazol-2-yl]thio]butyrate was obtained in a manner similar to Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933348 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-7f9b0b36f41c40dda153f86550a0df67 |
| Source note | uspto-grants-1990_06 |