HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-chlorophenoxy)pentan-1-ol → 5-(4-Chlorophenoxy)pentanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-chlorophenoxy)pentan-1-ol | HCID 2794897 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 5-(4-Chlorophenoxy)pentanal | HCID 23297122 | — |
Reaction Steps
To a suspension of 33 g (0.15 mmol) of pyridinium chlorochromate in 450 ml of methylene chloride is added 21.4 g (0.1 mol) of 5-(4-chlorophenoxy)-1-pentanol. The mixture is maintained with stirring for 3 hours, diluted with 900 ml of ethyl ether and stirred for an additional 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933365 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-4f8bf6b412074a09805a47b356bf6f6f |
| Source note | uspto-grants-1990_06 |