HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 131716429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 3-Thiazolidineacetic acid, 4-oxo-2-thioxo- | HCID 79793 | — |
| Reactant | HCID 15053501 | HCID 15053501 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131716429 | HCID 131716429 | — |
Reaction Steps
Following a procedure similar to that described in Example 1, the desired compound was prepared from 1.8 g of ethyl 2-[3-(2,4-difluorophenyl)ureido]thiazol-4-ylglyoxylate, 0.96 g of rhodanine-3-acetic acid, 0.5 g of ammonium chloride, 0.5 ml of 28% v/v aqueous ammonia and 30 ml of ethanol. The resulting product was a yellow powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-4f880869f9cd4b03b097ec1d414c8cdd |
| Source note | uspto-grants-1990_06 |