HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-[(2E)-3-(2-Anilinothiazol-4-yl)allylidene]-rhodanine-3-acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 3-Thiazolidineacetic acid, 4-oxo-2-thioxo- | HCID 79793 | — |
| Reactant | (2E)-3-(2-anilinothiazol-4-yl)acrylaldehyde | HCID 15053531 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-[(2E)-3-(2-Anilinothiazol-4-yl)allylidene]-rhodanine-3-acetic acid | HCID 86744031 | — |
Reaction Steps
Following a procedure similar to that described in Example 1, the desired compound was prepared from 0.4 g of (2E)-3-(2-anilinothiazol-4-yl)acrylaldehyde, 0.29 g of rhodanine-3-acetic acid, 0.22 g of ammonium chloride, 0.2 ml of 28% v/v aqueous ammonia and 10 ml of ethanol. The resulting product was a reddish-brown powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-c053da2e314a42239369e009cb1ff21d |
| Source note | uspto-grants-1990_06 |