Sodium Methoxide → HCID 74086212, compound

HRID 2107206Notes

Reaction equation

HRID 2107206 reaction equation
[C:1]1([CH:7]([NH:14][C:15]2[S:16][CH:17]=[C:18]([CH:20]=[C:21]3[S:25][C:24](=[S:26])[N:23]([CH2:27][C:28]([OH:30])=[O:29])[C:22]3=[O:31])[N:19]=2)[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[O-].[Na+:34]>C(O)C>[OH2:29].[C:1]1([CH:7]([NH:14][C:15]2[S:16][CH:17]=[C:18]([CH:20]=[C:21]3[S:25][C:24](=[S:26])[N:23]([CH2:27][C:28]([O-:30])=[O:29])[C:22]3=[O:31])[N:19]=2)[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Na+:34]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 545717655-(2-Diphenylmethylaminothiazol-4-ylmethylene)rhodanine--acetic acid

Product 1

HCID 74086212HCID 74086212, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Following a procedure similar to that described in Example 35, the desired compound was prepared from 200 mg of 5-(2-diphenylmethylaminothiazol-4-ylmethylene)rhodanine-3-acetic acid, 24.5 mg of sodium methoxide and 6 ml of ethanol. The resulting product was a yellow powder having the following physical properties.

Sources & evidence

ORD record
ord-84af591aefbe4ec5a2d99278214906c9
Source dataset
uspto-grants-1990_06
Patent number
US04933355

Reaction notes

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