Ammonia → HCID 54133193, 화합물

HRID 2107212노트

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HRID 2107212 반응식
[CH2:1]([NH:4][C:5]1[S:6][CH:7]=[C:8]([CH:10]=O)[N:9]=1)[CH:2]=[CH2:3].[S:12]1[CH2:18][C:16](=[O:17])[N:15]([CH2:19][C:20]([OH:22])=[O:21])[C:13]1=[S:14].[Cl-].[NH4+].N>C(O)C>[CH2:1]([NH:4][C:5]1[S:6][CH:7]=[C:8]([CH:10]=[C:18]2[S:12][C:13](=[S:14])[N:15]([CH2:19][C:20]([OH:22])=[O:21])[C:16]2=[O:17])[N:9]=1)[CH:2]=[CH2:3]

참가 물질

6

반응물 4

HCID 222AmmoniaHCID 25517Ammonium ChlorideHCID 797933-Thiazolidineacetic acid, 4-oxo-2-thioxo-HCID 150535762-Allylaminothiazole-4-carbaldehyde

생성물 1

HCID 54133193HCID 54133193, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

The reaction described in Example 1 was repeated, but using 3.0 g of 2-allylaminothiazole-4-carbaldehyde, 2.8 g of rhodanine-3-acetic acid, 2.1 g of ammonium chloride, 2.1 ml of 28% v/v aqueous ammonia and 70 ml of ethanol giving 3.3 g of the title compound as brown needles.

출처 및 근거

ORD 기록
ord-febfdaaf83784a8590db3263da409de4
출처 데이터셋
uspto-grants-1990_06
특허 번호
US04933355

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