HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl isothiocyanate → HCID 15053498, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl isothiocyanate | HCID 16480 | — |
| Reactant | Ethyl 2-(2-Amino-4-thiazolyl)-2-oxoacetate | HCID 4356513 | — |
| Solvent | Hexamethylphosphoramide | HCID 12679 | — |
| Product | HCID 15053498 | HCID 15053498 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 1, the desired compound was prepared from 5 g of ethyl 2-aminothiazol-4-ylglyoxylate, 6.35 g of p-chlorophenyl isothiocyanate and 30 ml of hexamethylphosphoric triamide. The resulting product was a yellow powder having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-62b9e49a62f74ca4afa1074d2588fcb6 |
| Source note | uspto-grants-1990_06 |