HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23047624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N,N-Diphenylcarbamic chloride | HCID 65741 | — |
| Reactant | Ethyl 2-(2-Amino-4-thiazolyl)-2-oxoacetate | HCID 4356513 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23047624 | HCID 23047624 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 13, the desired compound was prepared from 5 g of ethyl 2-aminothiazol-4-ylglyoxylate, 7 g of diphenylcarbamoyl chloride, 30 ml of triethylamine and 20 ml of dimethylformamide. The resulting product was a brown oil having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-74222de7b30f44b0aa9e7154831d3e88 |
| Source note | uspto-grants-1990_06 |