HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromopyruvate → Ethyl 2-[(2-methylphenyl)amino]-4-thiazolecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromopyruvate | HCID 66144 | — |
| Reactant | N-(2-Methylphenyl)thiourea | HCID 2787703 | — |
| Product | Ethyl 2-[(2-methylphenyl)amino]-4-thiazolecarboxylate | HCID 1284666 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 42, the desired compound was prepared from 20 g of o-tolylthiourea, 23 g of ethyl bromopyruvate and 200 ml of giving the desired compound as pale yellow prismatic crystals having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-da3135c3ccd34c7e8119818b079f7594 |
| Source note | uspto-grants-1990_06 |