HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate → 2-Allylaminothiazol-4-ylmethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-[(prop-2-en-1-yl)amino]-1,3-thiazole-4-carboxylate | HCID 7171906 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Allylaminothiazol-4-ylmethanol | HCID 15053559 | — |
Reaction Steps
The reaction described in Preparation 15 was repeated, but using 10 g of ethyl 2-allylaminothiazole-4-carboxylate, 2.7 g of lithium aluminum hydride and 150 ml of tetrahydrofuran. giving the title compound as pale brown needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-96b70246f9234f0a9c9bdb303be4c2c6 |
| Source note | uspto-grants-1990_06 |