HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178472284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | Phosphinic Acid | HCID 4124402 | — |
| Product | HCID 178472284 | HCID 178472284 | 64.5% |
Reaction Steps
Using the procedure described in Example 1b, 363 parts of 90% aqueous phosphinic acid solution are reacted with 1930 parts of triethyl orthoformate in the presence of 114 parts of trifluoroacetic acid. Work up and purification by the procedures of Example 1b gives 631.5 parts (64.5%) of ethyl diethoxymethylphosphinate of 96.9% purity.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933478 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-c02de58c550d4f8d8781cb6dfdcbfe91 |
| Source note | uspto-grants-1990_06 |