Sodium Hydroxide → HCID 23705008, compound

HRID 2107920Notes

Reaction equation

HRID 2107920 reaction equation
[C:1]1([C:7]2[N:15]([CH3:16])[C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[CH:13][C:12](=[O:23])[C:8]=2[C:9]([OH:11])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Na+:25]>CO>[C:1]1([C:7]2[N:15]([CH3:16])[C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=3)=[CH:13][C:12](=[O:23])[C:8]=2[C:9]([O-:11])=[O:10])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[Na+:25]

Participants

4

Reactant 2

HCID 14798Sodium Hydroxide2×HCID 14075370HCID 14075370, compound

Product 1

HCID 23705008HCID 23705008, compoundYield 94.4%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.73 gms of 2,6-diphenyl-1-methyl-4-oxonicotinic acid was suspended in 50 mls of dry methanol. 0.25 gms of NaOH was added. After the carboxylic acid and the NaOH dissolved the solvent was removed yielding 1.75 gms of sodium 2,6-diphenyl-1-methyl-4-oxonicotinate as a glassy solid.

Workup

  1. customwas removed

Sources & evidence

ORD record
ord-696efe6517494c26b79d9b9a262b5bf7
Source dataset
uspto-grants-1990_06
Patent number
US04936904

Reaction notes

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