Sodium Hydroxide → HCID 23705002, compound

HRID 2107922Notes

Reaction equation

HRID 2107922 reaction equation
[CH2:1]([N:3]1[C:11]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[CH:10][C:9](=[O:18])[C:5]([C:6]([OH:8])=[O:7])=[C:4]1[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH3:2].[OH-].[Na+:26]>CO>[CH2:1]([N:3]1[C:11]([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)=[CH:10][C:9](=[O:18])[C:5]([C:6]([O-:8])=[O:7])=[C:4]1[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[CH3:2].[Na+:26]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 14075371HCID 14075371, compound

Product 1

HCID 23705002HCID 23705002, compoundYield 94.9%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.38 gms of 1-ethyl-2,6-diphenyl-4-oxonicotinic acid was treated with 0.19 gms of NaOH in 50 mls of dry methanol. Evaporation of the solvent provided 1.40 gms of sodium 1-ethyl-2,6-diphenyl-4-oxonicotinate as a glassy solid.

Workup

  1. customEvaporation of the solvent

Sources & evidence

ORD record
ord-cb2664dc560f4242b7709a14c84fd445
Source dataset
uspto-grants-1990_06
Patent number
US04936904

Reaction notes

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