Sodium Hydroxide → HCID 23704998, compound

HRID 2107932Notes

Reaction equation

HRID 2107932 reaction equation
[CH2:1]([N:4]1[C:12]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:11][C:10](=[O:19])[C:6]([C:7]([OH:9])=[O:8])=[C:5]1[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[CH2:2][CH3:3].[OH-].[Na+:27]>CO>[CH2:1]([N:4]1[C:12]([C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)=[CH:11][C:10](=[O:19])[C:6]([C:7]([O-:9])=[O:8])=[C:5]1[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)[CH2:2][CH3:3].[Na+:27]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 14075379HCID 14075379, compound

Product 1

HCID 23704998HCID 23704998, compoundYield 93.8%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.5 gms of 1-propyl-2,6-diphenyl-4-oxonicotinic acid, 0.202 gms of NaOH and 50 mls of dry methanol were mixed. Evaporation of the solvent yielded 1.5 gms of sodium 1-propyl-2,6-diphenyl-4-oxonicotinate as a white glassy solid.

Workup

  1. customEvaporation of the solvent

Sources & evidence

ORD record
ord-3698cc631ace45558bbb995dd4b383d7
Source dataset
uspto-grants-1990_06
Patent number
US04936904

Reaction notes

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