1,6-Dibromohexane → HCID 23045084, compound

HRID 2108022Notes

Reaction equation

HRID 2108022 reaction equation
[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][CH2:9][OH:10])=[CH:3][CH:2]=1.[Br:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17]Br>>[Br:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][O:10][CH2:9][CH2:8][CH2:7][C:4]1[CH:5]=[CH:6][N:1]=[CH:2][CH:3]=1

Participants

3

Reactant 2

HCID 123681,6-DibromohexaneHCID 729234-Pyridinepropanol

Product 1

HCID 23045084HCID 23045084, compound

Procedure

From 4-pyridinepropanol (2.0 g) and 1,6-dibromohexane (8 ml), with a reaction time of 30 min. FCC eluting with hexane→ether gave the title compound as a colourless oil (1.1 g), t.l.c. (ether) Rf 0.45.

Workup

  1. customwith a reaction time of 30 min
  2. washFCC eluting with hexane→ether

Sources & evidence

ORD record
ord-acc2ea99cc1d4a1489249b5fa69b538e
Source dataset
uspto-grants-1990_06
Patent number
US04937251

Reaction notes

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