HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → HCID 23045080, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | Pyripropanol | HCID 72922 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23045080 | HCID 23045080 | 52.7% |
Reaction Steps
From 2-pyridinepropanol (5 g) and 1,5-dibromopentane (24.83 g), stirring the reaction mixture under nitrogen for 5 h, and using ethyl acetate for extraction. FCC eluting with cyclohexane→cyclohexane-ethyl acetate (9:1) gave the title compound as a yellow oil (5.5 g), t.l.c. (cyclohexane-ethyl acetate 9:1) Rf 0.15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04937251 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-349b7319ad3e4482b521f273deed8f8b |
| Source note | uspto-grants-1990_06 |