HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromotoluene → 3-(3-methylphenyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromotoluene | HCID 11560 | — |
| Reactant | 3-Bromopyridine | HCID 12286 | — |
| Reactant | 3-(3-methoxyphenyl)pyridine | HCID 4133193 | — |
| Product | 3-(3-methylphenyl)pyridine | HCID 4133190 | — |
Reaction Steps
3-(3-methylphenyl)-pyridine was prepared from 81.5 g (0.52 mol) 3-bromopyridine and 120 g (0.70 mol) 3-bromo-toluene as described for the preparation of 3-(3-methoxyphenyl)-pyridine. (Example I7.) B.p. 87° /0.05 mmHg. Yield 61.7 g (69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04937346 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-0d18303f844448348de8e13ba14a8fba |
| Source note | uspto-grants-1990_06 |