HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 44140827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 11198244 | HCID 11198244 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 44140827 | HCID 44140827 | — |
Reaction Steps
A mixture of compound 6 (0.25 g) and potassium carbonate (0.3 g) in methanol-water (15 ml, 9:1) was stirred at room temperature for 8 hr. Solution was concentrated diluted with cold water, cooled and the precipitated solid was filtered, and crystallized from methanol. White solid, mp. 138-40° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514420B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-06f27a32e6cc4bcebcbdf738eab0451e |
| Source note | uspto-grants-2009_04 |