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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2108363Generated: November 1, 2026

HCID 57629503, compound → HCID 57629486, compound

https://huagongshe.com/reaction/2108363

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57629503HCID 57629503—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 57629486HCID 5762948682%

Reaction Steps

A solution of 106B (50 mg, 0.15mmol) in MeOH (10 mL) was degassed for 10 minutes and then treated with 10% Pd on activated carbon (15 mg). The reaction mixture was stirred at room temperature for 18 hours under a hydrogen atmosphere. The catalyst was removed by filtration and the filtrate was concentrated to give 4-morpholino-2-(2-morpholinoethoxy)aniline (35 mg, 82%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07514435B2
Source datasetuspto-grants-2009_04
ORD IDord-49b6965c80df45ecb9454649351c7216
Source noteuspto-grants-2009_04