HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57629503, compound → HCID 57629486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57629503 | HCID 57629503 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57629486 | HCID 57629486 | 82% |
Reaction Steps
A solution of 106B (50 mg, 0.15mmol) in MeOH (10 mL) was degassed for 10 minutes and then treated with 10% Pd on activated carbon (15 mg). The reaction mixture was stirred at room temperature for 18 hours under a hydrogen atmosphere. The catalyst was removed by filtration and the filtrate was concentrated to give 4-morpholino-2-(2-morpholinoethoxy)aniline (35 mg, 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514435B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-49b6965c80df45ecb9454649351c7216 |
| Source note | uspto-grants-2009_04 |