Bromoacetyl bromide → HCID 57421976, compound

Participants

Reaction Steps

The title compound was synthesized in 2 steps in a manner similar to that described above using 5-chloro-7-azaindole (0.32 g, 1.17 mmol), AlCl3 (0.47 g, 3.51 mmol), bromoacetylbromide (0.1 mL, 1.46 mmol) and thiourea (0.158 g, 2.08 mmol) (0.21 g, 67.5%, 2 steps) as pale brown solid. Mass Spec.; MS 251 (M+1); 1H NMR(DMSO-d6, 500 MHz) δ 11.97(s, 1H), 8.50(d, 1H), 8.22(d,1H), 7.84(d,1H),7.02(brs,2H), 6.83(s,1H).

Provenance & Evidence