Bromoacetyl bromide → HCID 57421978, compound

Participants

Reaction Steps

The title compound was synthesized in 2 steps in a manner similar to that described above using 5-methoxy-7-azaindole (0.37 g, 2.48 mmol), AlCl3 (1 g, 7.54 mmol), bromoacetylbromide (0.2 mL, 3 mmol) and thiourea (0.14 g, 1.88 mmol) (0.21 g, 39%, 2 steps) as a brown solid. Mass Spec.; MS 233 (M+1); 1H NMR(DMSO-d6, 500 MHz) δ 11.37 (s,1H), 9.10(s,1H), 7.86(d,1H), 7.70(d,1H), 7.61(d,1H), 6.88(s,2H), 6.67(s,1H).

Provenance & Evidence