HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Anisoyl chloride → N-[2-(6,7-Dimethoxyquinazolin-4-ylamino)-benzothiazol-6-yl]-4-methoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | N2-(6,7-dimethoxyquinazolin-4-yl)benzothiazole-2,6-diamine | HCID 86248039 | — |
| Product | N-[2-(6,7-Dimethoxyquinazolin-4-ylamino)-benzothiazol-6-yl]-4-methoxybenzamide | HCID 11612819 | — |
Reaction Steps
N-[2-(6,7-Dimethoxyquinazolin-4-ylamino)-benzothiazol-6-yl]-4-methoxybenzamide was prepared from p-anisoyl chloride (16 μL, 0.113 mmol) and N2-(6,7-dimethoxyquinazolin-4-yl)benzothiazole-2,6-diamine (40 mg, 0.113 mmol) according to GP 2 (yellowish solid, 46 mg, 94 μmol, 83%). LC/ESI-MS: m/z=488 [M+H]+; m/z=486 [M−H]−; R′, =3.17 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514460B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-45716620014e4ccf825e5719bc2c3251 |
| Source note | uspto-grants-2009_04 |