HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Anisoyl chloride → HCID 11684531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Anisoyl chloride | HCID 74374 | — |
| Reactant | N2-(6,7-dimethoxyquinazolin-4-yl)benzothiazole-2,6-diamine | HCID 86248039 | — |
| Product | HCID 11684531 | HCID 11684531 | — |
Reaction Steps
N-[2-(6,7-Dimethoxyquinazolin-4-ylamino)benzothiazol-6-yl]-3-methoxybenzamide was prepared from m-anisoyl chloride (17 μL, 0.113 mmol) and N2-(6,7-dimethoxyquinazolin-4-yl)benzothiazole-2,6-diamine (40 mg, 0.113 mmol) according to GP 2 (yellowish solid, 41 mg, 84 μmol, 74%). LC/ESI-MS: m/z=488 [M+H]+; m/z=486 [M−H]−; Rt=3.17 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514460B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-0678aff10d9a4d6d8ff71cce045db1bd |
| Source note | uspto-grants-2009_04 |