3-(4-methylphenyl)-1H-indazole → HCID 24755955, compound

HRID 2108996Notes

Reaction equation

HRID 2108996 reaction equation
Cl[C:2]([C:4]1[CH:14]=[CH:13][C:7]([C:8]([O:10][CH2:11][CH3:12])=[O:9])=[CH:6][CH:5]=1)=O.CC1C=CC(C2[C:30]3[C:25](=[CH:26][CH:27]=[CH:28][CH:29]=3)[NH:24][N:23]=2)=CC=1>>[NH:24]1[C:25]2[C:26](=[CH:27][CH:28]=[CH:29][CH:30]=2)[C:2]([C:4]2[CH:14]=[CH:13][C:7]([C:8]([O:10][CH2:11][CH3:12])=[O:9])=[CH:6][CH:5]=2)=[N:23]1

Participants

3

Reactant 2

HCID 98777323-(4-methylphenyl)-1H-indazoleHCID 12276626p-Ethoxycarbonylbenzoyl chloride

Product 1

HCID 24755955HCID 24755955, compoundYield 88.9%

Procedure

Ethyl 4-(chlorocarbonyl)benzoate was treated as in the preparation of 10 to afford 11 (0.94 g, 88.9%).

Sources & evidence

ORD record
ord-c0e36842c4db4551b1588400a0ef923a
Source dataset
uspto-grants-2009_04
Patent number
US07514465B2

Reaction notes

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