HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethylhydrazine → 2-[4-Cyano(2,2,2-trifluoroethyl)-3-(trifluoromethyl)anilino]-N',N'-dimethylacetohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethylhydrazine | HCID 5976 | — |
| Reactant | N-[4-cyano-3-(trifluoromethyl)phenyl]-N-(2,2,2-trifluoroethyl)glycine | HCID 57633731 | — |
| Product | 2-[4-Cyano(2,2,2-trifluoroethyl)-3-(trifluoromethyl)anilino]-N',N'-dimethylacetohydrazide | HCID 11314632 | — |
Reaction Steps
Synthesized as described in example 3 using N-[4-cyano-3-(trifluoromethyl)phenyl]-N-(2,2,2-trifluoroethyl)glycine and 1,1-dimethylhydrazine: 1H NMR (400 MHz, CD3OD) δ 7.77 (d, J=9.6 Hz, 1H), 7.14 (bs, 2H), 7.08 (s, 1H), 4.36 (q, J=9.0 Hz, 2H), 4.26 (s, 2H), 2.69 (s, 3H), 2.61 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514470B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-42c365ccfe41451bb0c82e3ea72ea117 |
| Source note | uspto-grants-2009_04 |