HRID2109108

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID79177

Acetic acid, bromo-, 1,1-dimethylethyl ester

C6H11BrO2

HCID57633757

2-(Trifluoromethyl)-4-[(3,3,3-trifluoropropyl)amino]benzonitrile

C11H8F6N2

PRODUCTS

生成物

结构：CC(C)(C)OC(=O)CN(CCC(F)(F)F)c1ccc(C#N)c(C(F)(F)F)c1

HCID11749814

未命名化合物

PROCEDURE

实验过程

Synthesized as described in example 1B using 2-(trifluoromethyl)-4-[(3,3,3-trifluoropropyl)amino]benzonitrile and tert-butyl bromoacetate: 1H NMR (400 MHz, CDCl3) δ 7.64 (d, J=8.8 Hz, 1H), 6.84 (d, J=2.6 Hz, 1H), 6.73 (dd, J=8.8, 2.6 Hz, 1H), 4.03 (s, 2H), 3.74 (t, J=7.5 Hz, 2H), 2.57-2.45 (m, 2H), 1.45 (s, 9H).

WORKUP

后处理

customSynthesized