tert-Butyl 2-bromobutanoate → HCID 57633732, compound

HRID 2109129Notes

Reaction equation

HRID 2109129 reaction equation
[CH:1]1([CH2:4][NH:5][C:6]2[CH:7]=[C:8]([C:14]#[N:15])[C:9]([C:12]#[N:13])=[CH:10][CH:11]=2)[CH2:3][CH2:2]1.Br[CH:17]([CH2:25][CH3:26])[C:18]([O:20][C:21]([CH3:24])([CH3:23])[CH3:22])=[O:19]>>[CH:1]1([CH2:4][N:5]([C:6]2[CH:11]=[CH:10][C:9]([C:12]#[N:13])=[C:8]([C:14]#[N:15])[CH:7]=2)[CH:17]([CH2:25][CH3:26])[C:18]([O:20][C:21]([CH3:24])([CH3:23])[CH3:22])=[O:19])[CH2:2][CH2:3]1

Participants

3

Reactant 2

HCID 13124118tert-Butyl 2-bromobutanoateHCID 57633701HCID 57633701, compound

Product 1

HCID 57633732HCID 57633732, compound

Procedure

Synthesized in a manner similar to example 1B using 4-[(cyclopropylmethyl)amino]-1,2-benzenedicarbonitrile and tert-butyl 2-bromobutanoate: MS (ES) m/z 340 (M+1).

Workup

  1. customSynthesized in a manner similar to example 1B

Sources & evidence

ORD record
ord-591e6fd5dc3b47b0a00d5540301b3e71
Source dataset
uspto-grants-2009_04
Patent number
US07514470B2

Reaction notes

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