3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide → HCID 21097073, compound

HRID 2109217Notes

Reaction equation

HRID 2109217 reaction equation
[N:1]([C:4]1[CH:5]=[C:6]([CH:27]=[CH:28][C:29]=1[CH3:30])[C:7]([NH:9][C:10]1[CH:15]=[C:14]([C:16]([CH3:19])([CH3:18])[CH3:17])[CH:13]=[C:12]([NH:20][S:21]([CH3:24])(=[O:23])=[O:22])[C:11]=1[O:25][CH3:26])=[O:8])=[N+:2]=[N-:3].[C:31]1([S:37]([C:40]2[N:41]([CH3:47])[C:42]([C:45]#[CH:46])=[CH:43][N:44]=2)(=[O:39])=[O:38])[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1>>[C:31]1([S:37]([C:40]2[N:41]([CH3:47])[C:42]([C:45]3[N:3]=[N:2][N:1]([C:4]4[CH:5]=[C:6]([CH:27]=[CH:28][C:29]=4[CH3:30])[C:7]([NH:9][C:10]4[CH:15]=[C:14]([C:16]([CH3:18])([CH3:19])[CH3:17])[CH:13]=[C:12]([NH:20][S:21]([CH3:24])(=[O:22])=[O:23])[C:11]=4[O:25][CH3:26])=[O:8])[CH:46]=3)=[CH:43][N:44]=2)(=[O:38])=[O:39])[CH:32]=[CH:33][CH:34]=[CH:35][CH:36]=1

Participants

3

Reactant 2

HCID 210792023-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamideHCID 21097264HCID 21097264, compound

Product 1

HCID 21097073HCID 21097073, compound

Procedure

Example 36 was prepared from 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide and 2-benzenesulfonyl-5-ethynyl-1-methyl-1H-imidazole in the same manner as Example 15. ESI MS m/z 678 [C32H35N7O6S+H]+.

Sources & evidence

ORD record
ord-7a4f9297a20c44a485481df673974bf6
Source dataset
uspto-grants-2009_04
Patent number
US07514458B2

Reaction notes

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