Dimethylamine → HCID 21097279, compound

HRID 2109235Notes

Reaction equation

HRID 2109235 reaction equation
I.CNC(=N)SC.CNC.C(N1C[CH2:22][N:21]([C:24]2[N:28]([CH3:29])[C:27]([CH:30]=[O:31])=[CH:26][N:25]=2)[CH2:20]C1)C1C=CC=CC=1.C(N1C[CH2:43][N:42]([C:45]2[N:46]([CH3:52])[CH:47]=[C:48]([CH:50]=[O:51])[N:49]=2)[CH2:41]C1)C1C=CC=CC=1>>[CH3:20][N:21]([CH3:22])[C:24]1[N:28]([CH3:29])[C:27]([CH:30]=[O:31])=[CH:26][N:25]=1.[CH3:41][N:42]([CH3:43])[C:45]1[N:46]([CH3:52])[CH:47]=[C:48]([CH:50]=[O:51])[N:49]=1

Participants

6

Reactant 4

HCID 674DimethylamineHCID 21097256HCID 21097256, compoundHCID 21097257HCID 21097257, compoundHCID 178485204HCID 178485204, compound

Product 2

HCID 21097279HCID 21097279, compoundHCID 210972801192139-69-7

Procedure

2-Dimethylamino-3-methyl-3H-imidazole-4-carbaldehyde and 2-dimethylamino-1-methyl-1H-imidazole-4-carbaldehyde were prepared from 1,2-dimethyl-isothiourea hydroiodide and dimethylamine in the same manner as 2-(4-benzyl-piperazin-1-yl)-3-methyl-3H-imidazole-4-carbaldehyde and 2-(4-benzyl-piperazin-1-yl)-1-methyl-1H-imidazole-4-carbaldehyde (Example 57 and Example 58).

Sources & evidence

ORD record
ord-a598768dcf334123bce4146987a6d2aa
Source dataset
uspto-grants-2009_04
Patent number
US07514458B2

Reaction notes

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