3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide → Benzamide

HRID 2109253Notes

Reaction equation

HRID 2109253 reaction equation
C(N1C(C=O)=CN=C1C1CC1)(C)(C)C.N([C:18]1[CH:19]=[C:20]([CH:41]=[CH:42][C:43]=1C)[C:21]([NH:23]C1C=C(C(C)(C)C)C=C(NS(C)(=O)=O)C=1OC)=[O:22])=[N+]=[N-]>>[C:21]([NH2:23])(=[O:22])[C:20]1[CH:41]=[CH:42][CH:43]=[CH:18][CH:19]=1

Participants

3

Reactant 2

HCID 210792023-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamideHCID 21097313HCID 21097313, compound

Product 1

HCID 2331Benzamide

Procedure

Example 82 benzamide was prepared from 3-tert-butyl-2-cyclopropyl-3H-imidazole-4-carbaldehyde and 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide in the same manner as Example 39. ESI MS m/z 620 [C32H41N7O4S+H]+.

Sources & evidence

ORD record
ord-cbeed8d158814ab5af94c45801825aea
Source dataset
uspto-grants-2009_04
Patent number
US07514458B2

Reaction notes

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