HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Azido-4-methylbenzoic acid → 3-Azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methyl-phenyl)-4-methyl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Azido-4-methylbenzoic acid | HCID 17973091 | — |
| Reactant | 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide | HCID 21079202 | — |
| Reactant | N-(3-Amino-5-tert-butyl-2-methyl-phenyl)-methanesulfonamide | HCID 21097367 | — |
| Product | 3-Azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methyl-phenyl)-4-methyl-benzamide | HCID 21097304 | — |
Reaction Steps
3-Azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methyl-phenyl)-4-methyl-benzamide was prepared from 3-azido-4-methyl benzoic acid (US 04/102492) and N-(3-Amino-5-tert-butyl-2-methyl-phenyl)-methanesulfonamide in the same manner as 3-azido-N-(5-tert-butyl-3-methanesulfonylamino-2-methoxy-phenyl)-4-methyl-benzamide (Example 15).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514458B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-77bcacd4a29e4babbe3d8c4965e933ad |
| Source note | uspto-grants-2009_04 |