HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 70150-84-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Ethyl 3-furoate | HCID 69201 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 70150-84-4 | HCID 12292748 | — |
Reaction Steps
Ethyl 3-furancarboxylate (7.0 g) and hydrazine monohydrate (4.8 ml) in ethanol (10 ml) were heated at reflux while stirring for 6 hours. The solvent was evaporated under reduced pressure, and the thus-precipitated crystals were recrystallized from ethanol, thereby giving 3.2 g of the desire compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514452B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-76b8ed65192e48999c9b1110a39677d1 |
| Source note | uspto-grants-2009_04 |