Ethanol → HCID 23062491, compound

HRID 2109387Notes

Reaction equation

HRID 2109387 reaction equation
Br[C:2]1C=COC=1C(O)=O.C(O)C.[C:13]([O:17][C:18]([NH:20][C:21]1[CH:22]=[C:23]([CH:27]=[CH:28][C:29]=1[O:30][CH3:31])[C:24]([OH:26])=[O:25])=[O:19])([CH3:16])([CH3:15])[CH3:14]>CO>[C:13]([O:17][C:18]([NH:20][C:21]1[CH:22]=[C:23]([CH:27]=[CH:28][C:29]=1[O:30][CH3:31])[C:24]([O:26][CH3:2])=[O:25])=[O:19])([CH3:16])([CH3:15])[CH3:14]

Participants

5

Reactant 3

HCID 702EthanolHCID 6054793-Bromofuran-2-carboxylic acidHCID 27356323-[(tert-Butoxycarbonyl)amino]-4-methoxybenzoic acid

Product 1

HCID 23062491HCID 23062491, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A reaction and treatment was conducted in the same manner as in Reference Example 1 except that the 3-bromo-2-furancarboxylic acid and ethanol used in Reference Example 1 were replaced with 3-(tert-butoxycarbonylamino)-4-methoxybenzoic acid (5.00 g) and methanol (0.76 ml), respectively, thereby giving 5.51 g of methyl 3-(tert-butoxycarbonylamino)-4-methoxybenzoate.

Workup

  1. customA reaction and treatment

Sources & evidence

ORD record
ord-517dadd1b0d746b481a30e5a3a4051d1
Source dataset
uspto-grants-2009_04
Patent number
US07514452B2

Reaction notes

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