HCID 68862321, compound → HCID 68863478, compound

HRID 2109405Notes

Reaction equation

HRID 2109405 reaction equation
FC1C=C(C=CC=1OC)C(NNC(C1OC=C(C2C=CC=CC=2)C=1C1C=CC=CC=1)=O)=O.[NH2:33][C:34]1[CH:35]=[C:36]([CH:60]=[CH:61][C:62]=1[O:63]C)[C:37]([NH:39][NH:40][C:41]([C:43]1[O:44][CH:45]=[C:46]([C:54]2[CH:59]=[CH:58][CH:57]=[CH:56][CH:55]=2)[C:47]=1[C:48]1[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=1)=[O:42])=[O:38]>>[NH2:33][C:34]1[CH:35]=[C:36]([CH:60]=[CH:61][C:62]=1[OH:63])[C:37]([NH:39][NH:40][C:41]([C:43]1[O:44][CH:45]=[C:46]([C:54]2[CH:55]=[CH:56][CH:57]=[CH:58][CH:59]=2)[C:47]=1[C:48]1[CH:49]=[CH:50][CH:51]=[CH:52][CH:53]=1)=[O:42])=[O:38]

Participants

3

Reactant 2

HCID 68862321HCID 68862321, compoundHCID 68864000HCID 68864000, compound

Product 1

HCID 68863478HCID 68863478, compoundYield 96.2%

Procedure

A reaction and treatment was carried out in the same manner as in Example 32 except that the compound of Example 31 used in Example 32 was replaced with the compound of Example 41 (1.00 g), thereby giving 0.93 g of the desired compound. Melting point: 268-270° C. (Recrystallized from methanol)

Workup

  1. customA reaction and treatment

Sources & evidence

ORD record
ord-8f31a7dfcbe4487494cdcc9060a32aeb
Source dataset
uspto-grants-2009_04
Patent number
US07514452B2

Reaction notes

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